Organic Chemistry lab

Eight 20.0 mmol of isopentyl alcohol into a 10 ml round off bottom flask match magnetic stir interdict Add 2.3 ml of glacial acetic stifling whence stir the mixutre Add .15 ml of concentrated sulfuric acid Connect a peeing cooled condenser to the chemical reaction flask figure out on the alter water and heat Reduce the heating rate if the reflux family rises to at bottom 2cm of the top of the condenser When the reaction time is up allow for the reaction mixture to cool to nearly room temperature. chip off the cooling water and remove the condenser with a few drops of water Transfer the reaction mixture to a love cap cartridge remover tube and add 6 ml of after using some of the after for the off Ash the reaction mix with the after and remove cautiously Pressure may build up in the caped centrifuge tube During the first washables stir the layers until gas phylogenesis subsides before you cap the centrifuge tube and vent it a great deal Try to remov e all of the sedimentary layer after the last washing to minimize the hail of water in the product Dry the crude isopentyl acetate by adding a small amount of anhydrous sodium sulfate carefully transfer the fluidness to a dry 5ml conical phial using a dry filter tip pipet Try not to transfer any drying agent with the liquid M.W b.p d solubility Acetic acid 60.

1 118 1.049 compatible Isopentyl alcohol 88.1 130 0.815 2.7 Isopentyl acetate 130.2 142 0.876 0.25 sulphuric acid ! 98.1 290 1.84 miscibleIf you compliments to get a full essay, revise it on our website: OrderEssay.net

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